地下水分析检测及质量控制

    Groundwater analysis, testing, and quality control

    • 摘要: 地下水分析检测方法的选择和检测过程中质量控制是地下水检测任务中重要的两个环节,其中涉及的方法很多,对应的标准也很多. 为提高工作效率、保证分析质量,本文对地下水标准体系、常用的地下水分析标准方法和质量控制方法进行梳理和介绍,以便在工作中更好地选择适合的检测方法、完成质量控制. 依托全国标准信息公共服务平台,查询了现行的可应用在地下水分析检测工作中的国家标准102份,行业标准311份(地方标准未纳入查询范围中). 这些标准从内容上包括地下水环境技术规范、地下水质量标准和地下水分析方法标准. 结合标准内容及测试工作经验,归纳介绍了常用的地下水分析方法,包括滴定法、光学分析法、电化学分析法、色谱分析法和质谱分析法. 质量控制方法的介绍主要是从检测方法选择、标准溶液溯源、分析过程中质量控制和测试数据正确性判断4个方面进行概述和探讨. 希望本文能对检验人员的地下水分析检测工作提供借鉴和帮助,能更好地支撑我国的地下水生态环境保护工作.

       

      Abstract: The selection of groundwater analysis and testing methods, along with quality control during the testing process, constitute two critical aspects of groundwater testing. These tasks involve a wide range of methods and an equally extensive array of standards. To improve work efficiency and ensure analytical quality, this paper provides an overview of the groundwater standard system, commonly used standard analytical methods for groundwater, and quality control approaches, to facilitate the selection of appropriate testing methods and the implementation of quality control in practice. Using the National Standard Information Public Service Platform, 102 current national standards and 311 current industry standards applicable to groundwater analysis and testing were identified (local standards were not included in the search). These standards cover technical specifications for the groundwater environment, groundwater quality standards, and analytical method standards. Based on the standard texts and practical testing experience, this paper summarizes commonly used groundwater analytical methods, including titration, optical analytical methods, electrochemical analysis, chromatographic analysis, and mass spectrometry. The discussion of quality control methods primarily focuses on four aspects:selection of testing methods, traceability of standard solutions, quality control during analysis, and validation of test data. This paper is intended to provide a reference for analysts engaged in groundwater testing, thereby supporting the protection of China's groundwater ecological environment.

       

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